3.无机非金属材料的制备.ppt

HRTEM image of the graphitic lattice near the surface of a sphere. The inset shows the SAED pattern from the near-surface of a sphere. 3~6层弯曲近平行的2~4 nm长 弧形图案测算，d=0.343 nm,  对应(002)晶面 弧形－曲率造成的 2900?C石墨化处理后碳球发生多面体转变(a) SEM像, (b) TEM像 结果与分析 330?50 nm 同一多面体粒子不同部位 石墨烯层平行于入射电子束 0.340~0.344 nm 0.3354 nm “脊梁区” 高角晶界 越心部越薄 Thermogravimetric analysis of the carbon spheres heated in air at 10?C/min 结果与分析 XRD pattern of the carbon spheres after heat treatment at 2100?C 结果与分析 Qiu et. al, Carbon,2003,41:767-772 (10) (004) (10) (11) (004) (002) Cycle times versus capacity of (a) the as-synthesized c