《毕业设计(论文)-二氧化硅微粉制备工艺设计》.doc

攀枝花学院本科毕业设计（论文）学生姓名：学生学号：院（系）：年级专业： 200级材料科学与工程 指导教师： 助理指导教师：二〇年六 mol/L硅酸钠储备液，0.4 mol/L的硫酸反应，同时加入1mol/L NaCl添加剂， 150mg/L超分散剂聚乙二醇，温度控制在50±5℃，反应时间为45min后，加0.5mol/L的硫酸至pH值在5～6除去非金属化合物，中和反应体系残余的碱；在40～50℃温度下恒温陈化100min 使体系中的粒子比较均匀，自然长大为凝胶。用离心法反复分离料浆洗涤去除杂，置于105±5℃烘箱中干燥，用超音速气流粉碎机粉碎微粉出现团聚结块现象，得到高质量的二氧化硅微粉。 关键词 水玻璃，改良沉淀法，二氧化硅微粉ABSTRACT Because of its fine powder silica tensile strength，no staining residue, acid corrosion, thermal conductivity sent, stable in chemical, hardness etc, excellent performance in industrial production in a wide range of applications, so the Si02 micro powder is very necessary. This paper focuses on the silica micro powder, introduces the performance of silica micro powder production process and process optimization design. Optimization of silica micro powder production process for: in traditional precipitation added Chen hua. How do you do processes, changed charging, removing impurity, crushing process, use effect better additives and dispersant. Improved precipitated silica micro-powder parameters for the production of sodium silicate reserve liquid match: into PH=8±0.4 to join the reaction kettle, filling, degrees for 70%, 0.4 mol/L sodium silicate reserve liquid, 0.4 mol/L, add the sulfuric acid 1mol/L NaCl additives, 150mg/L super dispersant polyethylene glycol, temperature control in 50 ± 5 ℃, reaction time for 45min later add 0.5 mol/L sulfuric acid to pH in 5 ~ 6 remove nonmetal compounds, residual alkali neutralization reaction system; In 40—50 ℃ temperature constant temperature 100min make system in China grew up, natural relatively even particles to gel. Using centrifugation repeated separation pulp washing to remove all 105 ℃, on the plus or minus 5 in drying oven with supersonic airflow crusher, crushing micro-powder appear reunion agglomerate phenomenon, get high quality silica micro powder.Key words sodium silicate, improved precipitation, silica dioxide 目 录 摘 要 I ABSTRACT II 1 前言 1 2 二氧化硅微粉的结构与特性 2 2.1 纳米粒子的结构与特性