Pyris1TGA操作規范.docVIP

1.0 目的 PURPOSE 1.1 本规范描述了PE Pyris 1热失重分析仪的操作，校正和维护方法。 This document contains instructions used to provide a uniform method of operating, calibrating, and maintaining the Perkin Elmer Pyris 1 Thermogravimetric Analyzer. 2.0 范围 SCOPE 2.1 本规范包括Perkin Elmer Pyris 1 TGA的校验，操作，维护程序。 This document covers the calibration, operation, and maintenance procedures for the Perkin Elmer Pyris 1 TGA. 3.0 职责 RESPONSIBILITIES 3.1 所有的实验室分析人员必须遵守本规范。 This instruction should be observed by all testing personnel. 3.2 分析人员使用前应先检查设备的校验日期，如果过期，则应向实验室主管或QC校验人员汇报。 Visually check to make sure the calibration date on the instrument is not expired. If the instrument is expired, report it to a supervisor or the quality control calibration staff. 3.3 当仪器出现异常时应向实验室主管或QC校验人员汇报。 Malfunctioning instruments should be reported to both a supervisor and a QC calibration staff. 4.0 安全防护 SAFETY PRECAUTION 4.1 按管理要求穿戴合适的个人防护用品。 It is necessary to wear all Personal Protective Equipment assigned by your Supervisor. 4.2 预防措施Instrumental Precaution 注意：操作者在使用Pyris 1时必须遵守下面的预防措施： NOTE: The following precautions must be observed when using the Pyris 1 Thermogravimetric Analyzer. 4.2.1 当Pyris软件出现异常时不要按下计算机的Reset键。如果要关闭异常的Pyris窗口时应同时按下Ctrl+Alt+Del键，然后从任务管理其中关闭Pyris软件。 Never press the Reset button on the computer if the Pyris software appears to malfunction. Press the Ctrl-Alt-Del keys simultaneously and select the Task Manager. From the Task Manager, close the Pyris software. 4.2.2 在关闭PE Pyris 1设备和切断电源前，不要拆掉仪器上的任何面板。 Never remove the outer instrument cover or side panels on the PE Pyris 1 without shutting the instrument down and disconnecting its power cord from the power source. 4.2.3 PE Pyris 1所使用的气体纯度不应低于99.9%。 Only high-quality purge gases should be used with the PE Pyris 1. Minimum purity of 99.9% is recommended. 4.2.4 遵守PE Pyris 1和相关设备的开启和关闭程序。 Always observe the proper startup or shutdown procedures with the PE Pyris 1 and all related instruments. 4.2.5 通过天平室的气流流速始终控制在40-60cc/min, 建议使用惰性气体来作为天平室