氧化亚铜XRD测量数据.doc

寻峰报表(5个峰标,最大峰噪比=11.8) [07125-20.mdi] DX-2700 CSC 35kV/25mA Slit:1deg1deg.2mm Monochromator: ON Ts-Td 寻峰: 9(点)/四次项筛选,阈值=5.5,下限=0.1%,背景=3/1.0,峰标=峰顶法 2θ d(埃) 背景 峰高 峰高% 面积 面积% 半峰宽 晶粒(埃) 36.7420 2.4441 51.3 599.7 100.0 1336.3 100.0 0.284 370 42.6642 2.1175 72.8 215.2 35.9 330.5 24.7 0.184 735 61.7839 1.5003 72.0 208.0 34.7 399.7 29.9 0.245 504 73.9729 1.2804 66.4 116.6 19.5 310.7 23.3 0.340 349 77.9345 1.2249 60.2 31.8 5.3 39.1 2.9 0.150 1000 PDF#04-003-6433(RDB):质标=定胞(I);d=计算值;I=计算值 Cuprite, syn(Copper Oxide) Cu2 O 射线=CuKa1 波长=1.5406 滤波法= 校准= 2θ=29.7037-140.7057 I/Ic(K值)=8.07 文献: Pinsker Z.G., Imamov R.M. Sov. Phys. Crystallogr. (Engl. Transl.), v9 p334(1964) 立方晶系-(未知),Pn-3m(224) Z=2 晶胞: 4.25x4.25x4.25 90.0x90.0x90.0 P.S=cP6.00 密度(计算)=6.19 密度(测量)= 分子量=143.09 体积=76.77 F(20)=999.9(0.0002,20/0) 文献: 出处同上 强峰线: 2.45/X 2.13/3 1.50/3 1.28/2 3.01/1 ANX: A2X. LPF Collection Code: 457773. Sample Preparation: Compound Preparation: vaporization of Cu wire under vacuum followed by condensation of freshly cleaved surfaces of rocksalt. Sample annealed at 433-443 K. Minor Warning: Magnitude of e.s.d. on cell dimension is 1000 ppm. Unit Cell Data Source: Electron diffraction. 2θ d(埃) I(f) ( h k l) θ 1/(2d) 2π/d n^2 29.7037 3.0052 5.4 ( 1 1 0) 14.8519 0.1664 2.0908 2 36.5921 2.4537 100.0 ( 1 1 1) 18.2960 0.2038 2.5607 3 42.5066 2.1250 34.3 ( 2 0 0) 21.2533 0.2353 2.9568 4 52.7135 1.7351 1.1 ( 2 1 1) 26.3567 0.2882 3.6213 6 61.6799 1.5026 25.4 ( 2 2 0) 30.8399 0.3328 4.1815 8 65.8767 1.4167 0.1 ( 2 2 1) 32.9384 0.3529 4.4352 9 69.9402 1.3440 0.3 ( 3 1 0) 34.9701 0.3720 4.6751 10 73.9012 1.2814 18.4 ( 3 1 1) 36.9506 0.3902 4.9033 11 77.7839 1.2269 3.9 ( 2 2 2) 38.8920 0.4075 5.1213 12 85.4001 1.1359 0.2 ( 3 2 1) 42.7000 0.4402 5.5317 14 92.9350 1.0625 2.1 ( 4 0 0) 46.4675 0.4706 5.9136 16 96.7129 1.0308 0.1 ( 3 2 2) 48.3565 0.4851 6.0956 17 100.5220 1.0017 0.1 ( 4 1 1) 50.2610 0.4991 6.2723 18 104.3771 0.9750 4.7 ( 3 3 1) 52.1885 0.5128 6.4442 19 108.3006 0.9503 3.4 ( 4 2 0) 54.1