zno纳米tio2复合粉体材料.doc

ZnO/纳米TiO2复合粉体材料 的制备研究 摘 要 纳米TiO2和纳米ZnO粉体具有优异的紫外线吸收性能，TiO2/ZnO复合粉体。 由于这种复合粉体具有无机抗紫外线剂的优良性能，而又具有比其它无机抗紫外线剂更优异的性能。因此，其制备及应用的研究受到广泛的关注。TiO2/ZnO复合粉体。 本文以H2TiO3浓缩液为原料来制备硫酸氧钛溶液，以碳酸钠溶液为沉淀剂来制备出Ti(OH)4沉淀，再利用ZnCO3沉淀来包覆Ti(OH)4沉淀，并在适当的温度下进行煅烧，得到样品。将得到的样品利用XRD进行样品中物相的分析，用激光粒度仪进行样品的粒度分布分析，用TEM对样品进行颗粒形貌分析，用紫外线吸收仪所对样品的抗紫外线性能进行了测试分析。分析表明，本研究最终成功地制得了纳米TiO2/ZnO复合粉体。研究表明，复合粉体的粒径在20nm～50nm 纳米TiO2/ZnO ABSTRACT Nanometer TiO2 and the nanometer ZnO powder has the outstanding ultraviolet absorption performance, but sole powder has certain insufficiency when it is being used. Moreover, the sole powder can appear the pulverization when it is being used, and get waits in vain the phenomenon. This article unified two kind of powder merit, have prepared one kind compound powder which has outstanding ultraviolet absorption performance - - nanometer TiO2/ZnO compound powder. Because this kind of compound powder has fine performance that is the inorganic anti-ultraviolet medicinal, and therefore, has more outstanding performance compared to other inorganic on anti-ultraviolet medicinal. Therefore, its preparation and the application research receives the widespread attention. The domestic and foreign researches have already acquired the corresponding results, and have carried on some simple reports with its preparation method. Through various research, we had found one both simple and economy, also the environmental protection technique co-precipitation prepare nanometer —nanometer TiO2/ZnO compound powder. This article take the H2TiO3 concentrated solution as raw material prepares the titanyl ＿sulfate solution,　prepares the Ti(OH)4 precipitation take the sodium carbonate solution as the precipitating agent, then using ZnCO3 precipitates to wrapped Ti(OH)4 precipitation, and calcining under the suitable temperature, obtaining the sample. The obtained sample should be carried on the sample’s phase analysis with XRD, on the sample’s grain-size distribution analysis with t