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Photoresists The University of Oklahoma Department 光致抗蚀剂俄克拉何马大学
OU NanoLab/NSF NUE/Bumm Johnson ACTFEL Alternating Current Thin Film Electroluminescent Lamps Objective Use photolithography to pattern ITO Develop photoresist and etch ITO Apply layers of phosphors, dielectric, and silver Power up lamp Troubleshoot Preparation and Priming Prepare the substrate (glass, with ITO): Wash with appropriate solvent to remove any dirt and other impurities Acetone, MeOH Dry with Nitrogen Deposit Primer Chemical that coats the substrate and allows for better adhesion of the resist, HMDS Spin-Coating the Resist Spin-coat the photoresist onto the surface of the glass RPM: 4500 Time: 42 sec Produces a thin uniform layer of photoresist on the glass surface. Use red/amber safe light at this stage Soft-Baking Put on hotplate Temperature: 115°C, Time: 5 min Removes volatile solvents from the coating Makes photoresist imageable Hardens to amorphous solid Be careful not to overbake and destroy the sensitizer Be careful not to not soft-bake Mask Alignment and Exposure Photomask is a square piece of transparency printed on by a laser printer Maximize light intensity using photo-detector Remove all shadows from exposure area After alignment, the photoresist is exposed to the UV lamp Photoresist Developer Highly pure buffered alkaline solution Removes proper layer of photoresist upon contact or immersion Degree of exposure affects the resolution curves of the resist Immerse wafer in developer and swirl around for 90 seconds Wash developed wafer with deionized water and dry with nitrogen Etching the ITO Put glass in a beaker of 20% HCl, 5% HNO3 Heat beaker for 10 minutes in water bubble bath Check for infinite resistance across The Gap Fix Gap with razor blade if necessary Remove wafers and wash in acetone Dry with Nitrogen Applying Thin Films After the ITO is patterned the ACTFEL lamp can be made. Each layer comes packaged separately as a thick paste (stir before using). The thickness of each layer is controlled by using scotch tape as a spacer. Ap
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