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2015-Low temperature synthesis of forsterite from hydromagnesite and fumed silica mixture.pdf

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2015-Low temperature synthesis of forsterite from hydromagnesite and fumed silica mixture

CERAMICS INTERNATIONAL Available online at 0272-8842/ 20 nCorrespondin Leuven, Leuven E-mail addre(2015) 2234–2239Ceramics International 41 /locate/ceramintLow temperature synthesis of forsterite from hydromagnesite and fumed silica mixture Liugang Chena,b,n, Guotian Yea, Qingfeng Wanga, Bart Blanpainb, Annelies Malflietb, Muxing Guob aSchool of Materials Science and Engineering, Zhengzhou University, Zhengzhou 450001, China bDepartment of Materials Engineering, KU Leuven, Leuven BE-3001, Belgium Received 14 September 2014; received in revised form 2 October 2014; accepted 2 October 2014 Available online 13 October 2014Abstract Forsterite was prepared via solid-state reaction by using hydromagnesite (basic magnesia carbonate) and fumed silica, aiming at completing the reaction 2MgOtSiO2-Mg2SiO4 at low calcination temperature. The phase development and morphology evolution of the hydromagnesite and hydromagnesite–fumed silica mixture during heat treatment were characterized by means of scanning electron microscopy (SEM), Brunauer– Emmett–Teller (BET) nitrogen-gas adsorption method, and X-ray powder diffraction (XRD). A diffusion distance of less than 300 nm for Mg2t and Si4t for forsterite formation was obtained because the formed high reactivity MgO with the nanosheet structure of its parental hydromagnesite and the fumed silica with particle size of less than 100 nm were homogeneously mixed. Monolithic forsterite was synthesized after calcination of the hydromagnesite–fumed silica mixture at 1100 1C. 2014 Elsevier Ltd and Techna Group S.r.l. All rights reserved. Keywords: A. Calcination; A. Powders: solid state reaction; B. Electron microscopy; D. Silicate1. Introduction Forsterite (2MgO SiO2) has a high melting point (1890 1C), high temperature creep resistance, low thermal conductivity, and thus excellent insulation properties [1,2]. Therefore, forsterite is of interest to the high temperature ceramic industry [2,3]. Besides, forsterite-based ceramics can als