ELPI设定条件对卷烟主流烟气气溶胶检测结果的影响.pdfVIP

2016 年 2 月 烟草科 技 Feb. 2016 第 49 卷 第 2 期 Tobacco Science Technology Vol. 49 No. 2 ELPI 设定条件对卷烟主流烟气气溶胶检测结果的影响 孔浩辉，吴君章，沈光林* 88 510385 广东中烟工业有限责任公司，广州市荔湾区东沙环翠南路 号 摘要：为准确测定卷烟主流烟气气溶胶的粒径分布，建立了“分流+轴向稀释器+20 倍射流稀释器”的电 子低压撞击器(ELPI)的配套稀释系统和相应的检测方法，并对 19 个不同焦油量(7.79~12.88 mg/支)的卷 烟样品进行检测。结果表明：①采用该稀释系统，可满足 ELPI 分析仪在测定卷烟主流烟气气溶胶过程 中对检测稳定性和仪器检测限的要求。②采用该 ELPI 方法检测卷烟烟气气溶胶时，测试时间对检测结 果的影响较小，组间相对标准偏差(RSD)＜10%。③该方法的稳定性良好，气溶胶总质量检测结果的 RSD＜15%。该方法准确、稳定和可靠，适用于不同焦油量卷烟样品烟气气溶胶颗粒的检测。 ELPI 关键词：卷烟；主流烟气；气溶胶；粒径分布； ；稀释系统 - - - 中图分类号：TS411.2 文献标志码：A 文章编号：1002 0861（2016）02 0062 06 Influences of ELPI conditions on test results of mainstream cigarette smoke aerosol KONG Haohui, WU Junzhang, SHEN Guanglin* China Tobacco Guangdong Industrial Co., Ltd., Guangzhou 510385, China Abstract: In order to accurately determine the particle size distribution in mainstream cigarette smoke aerosol, a dilution system, which was composed of a diverter, an axial diluter and a 20 times jet-flow diluter, and the corresponding detection method for electrical low pressure impactor (ELPI) instrument were established. The experimental results indicated that: 1) The dilution system met the requirements of ELPI for detection stability and instrument detection limits in the determination of mainstream cigarette smoke aerosol. 2) The influence of test time on the test results was minor when detecting smoke aerosol with this ELPI-based method, and the inter-assay relative standard deviation (RSD) was less than 10%. 3) This method featured a good stability, and