An Extraction Technique of asthma.docVIP

 PAGE \* MERGEFORMAT 12 An Extraction Technique of asthma [Abstract] Objective To optimize the extraction of particles An asthma. Methods for the Evaluation of ephedrine hydrochloride, the choice of orthogonal test, study 6 ephedra and other herbs in the water in the water extraction, extraction time and extraction times on the hydrochloric acid Ephedrine effects of matrine, oxymatrine content evaluation, study, etc. 2 flavescens flavor extraction of drugs in the concentration of alcohol, ethanol, extraction time and extraction times of matrine and oxidation matrine content. The results determine the best option is: 6 flavored herbs such as ephedra boiling water 2 times, each time 2 h, 1st Add 854 mL, 2 times plus 732 mL, 2 flavor and other herbs flavescens and 80% ethanol extract 2 times 2 h, 1st Add 288 mL, 2 times plus 240 mL. Conclusion The optimized extraction process is reasonable, practical, quality control. [Keywords: An asthma particles, experiment, ephedrine hydrochloride, matrine, oxymatrine, high performance liquid chromatography Keywords:: Anchuan Keli, orthogonal test, ephedrina hydrochloridum, matrine, ammothamnine, HPLC An original prescription from asthma particles Jiangsu Province Hospital of Integrated Traditional and Western Respiratory Zhuqi Yong, director of clinical prescription, from ephedra, plum, licorice, Sophora composed of 8 herbs. On Treatment of asthma has a significant effect of bronchial asthma. In order to overcome the original square decoction and use the more complicated the larger the amount of the deficiency of the development of the parties. In this study, orthogonal to the extraction process were optimized. l equipment and materials AL204 millionth electronic balance (Mettler company’s products), Agilent 1100 HPLC (Agilent American products), DAD detector, Agilent Chemstation chromatography data workstation. Ephedrine hydrochloride (batch 171241-200303) reference substance matrine (Lot 0805-970) referenc