Astragalus from different habitats in the study of organochlorine pesticide residues in.docVIP

 PAGE \* MERGEFORMAT 15 Astragalus from different habitats in the study of organochlorine pesticide residues in 【Abstract】 Objective To evaluate the different origin of the astragalus of organochlorine pesticide residues in medicinal quality evaluation. Methods  water extraction system, acetone, dichloromethane liquid-liquid distribution, concentrated sulfuric acid sulfonation purification technology, flexible quartz capillary column (30 m × 0.32 mm × 0.25 μm) SE  54, GC  ECD detection of organochlorine pesticide residues . Results The minimum detection limit is 0.1 ~ 0.5ng / g, the recovery was 72.6% ~ 114.8%; Gansu, Inner Mongolia and other main origin of organochlorine pesticide residues in Astragalus is far below the “Chinese Pharmacopoeia” standard. Conclusion A set of simple, workable detection of Radix Astragali organochlorine pesticide residues analysis. Keywords: capillary gas chromatography; organochlorine pesticides; Astragalus; residues Study on Residues of Organochlorine Pesticides in Radix Astragali Samples from Different Field Origins Abstract: ObjectiveTo program a quality evaluation of organochlorine pesticides residue on Radix Astragali produced from different places. MethodsSonication extraction system was used, in which acetone was the extractant. Based on salting out principles, sodium chlorine was added to the extractant to separate the pesticides. Simultaneously, CH2Cl2 was also added to carry out liquid extraction, then it was purified by dense sulphuric acid, and finally detected by GC  ECD. ResultsThe detection limits were 0.1 ~ 0.5 ng / g, recoveries of organochlorine pesticides were 72.6% ~ 114.8% . Radix Astragali produced from Gansu, Neimeng ect were more lower than the standard of pharmacopeia.ConclusionA simple and handling analytical method to detect the organochlorine pesticides of Radix Astragali has been established. Keywords:: Capillary gas chromatography; Organochlorine pesticides;