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Chinese herbal compound pharynx bian syrup formulation of quality standards
Authors: Xiao cited, Ma Yongzhi, Lü Jie, Li Bo, Xiong Xiao-Jun
[Abstract] Objective: To establish the pharyngeal bian Syrup quality standards. Methods: The thin-layer chromatography prescriptions Ophiopogon, honeysuckle qualitative identification, high-performance liquid chromatography sample the content of baicalin, using C18 column ( 4.6 mm * 150 mm, 5 μ m), mobile phase: methanol 2 g / L phosphoric acid (40:60); detection wavelength 280 nm; flow rate 1 mL / min. Results: The TLC identification method of specific, negative control without interference; assay results showed that baicalin sample volume in the range of 0.1405 ~ 1.2641 μ g good linear relationship (r = 0.9998), the average recovery was 98.71%, RSD of 0.52% (n = 5). Conclusion: thin-layer chromatography method is accurate, simple, specific and reproducible, and can be used for quality control of the pharyngeal bian syrup.
[Keywords:] Pharyngeal bian syrup; chromatography, thin layer; chromatography, high pressure liquid; baicalin; quality standards
[Abstract] AIM: To establish the quality standard for Syropus Yan Bian. METHODS: Radix Ophiopogonis, Honeysuckle Flower in Syropus Yan Bian were identified by thin layer chromatography (TLC). The baicalin cotent was determined by high performance liquid chromatography (HPLC) on C18 column (5 μ m, 4.6 mm * 150 mm), with a mobile phase of methanol 2 g / L phosphoric acid (40:60). The flow rate was 1.0 ml / min, and the detection wavelength was set at 280 nm. RESULTS: Radix Ophiopogonis and Veitchii Lynch were identified by TLC. The calibration curve was in good linearity over the range of 0.1405-1.2641μ g (r = 0.9998). The average recovery rate was 98.71%, and RSD was 0.52 % (n = 5). CONCLUSION: The method is simple, reliable and accurate, and it can be used for quality control of Syropus Yan Bian.
[Keywors] syropus yan bian;
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