Determination of post-partum on the posted content of caffeic acid wipes.docVIP

 PAGE \* MERGEFORMAT 8 Determination of post-partum on the posted content of caffeic acid wipes [Abstract] Objective Determination of the establishment of post-paste of caffeic acid content in wet tissue. Methods column was HangBang C18 (200 mm × 4.6 mm, 5 μm), mobile phase was methanol - phosphate buffer ( 23:77), detection wavelength was 323 nm, flow rate 1.0 mL / min, injection volume was 10 μL. the results of testing the concentration of caffeic acid in the linear range of 0.052 ~ 0.26 μg (r = 0.999 8), the average recovery was 97.44% (RSD = 0.78%). Conclusion The method is simple, rapid, accurate, and can be used for the preparation of quality control. [Keywords:] post-paste wipes, high performance liquid chromatography, caffeic acid, determination Keywords:: Chanhou Tieshijin; HPLC, caffeic acid, content determination Post postpartum wipes (hospital preparation) is a dandelion, frankincense, dragon’s blood, Duan keel, safflower, Chi Shizhi, borneol, etc. decoction alcohol precipitation, concentration, non-woven fabrics made of medicated wipes invasion. Wet each piece size stickers postpartum 4.5 cm × 7 cm, water content of 5 mL, each affixed to a weight of 10 g, used in wound healing after episiotomy suture. The test of post-paste the content of caffeic acid wipes determination for its quality control. are reported below. An instrument and reagent Waters HPLC, Waters2487 UV detector (U.S. Waters 515), Hangzhou, English HS chromatography data workstation spectrum technology V4.0 + (Child Health Hospital of Nanjing preparation room), AE100 electronic analytical balance (Mettler - Toledo Instrument Co., Ltd.). caffeic acid reference substance by the Pharmaceutical and Biological Products, provided (used for content determination, batch number 110885-200102), posted wipes for the hospital post-natal preparation (batch 070603,070826,070924,071025) . chromatogram of pure methanol, sodium dihydrogen phosphate, phosphoric acid of analytical grad