High Performance Liquid Chromatography Gukang Oral psoralen and isopsoralen content.docVIP

 PAGE \* MERGEFORMAT 10 High Performance Liquid Chromatography Gukang Oral psoralen and isopsoralen content Author: Zhong Jing Jin Huang Qi-Long Ren Yan-Gang Zeng Hui-fang Su [Abstract] Objective To establish a bone-kang oral liquid in the method for determination of the active ingredient. Methods HPLC determination of bone-kang oral liquid content of the active ingredient. Results psoralen and Isopsoralen two kinds of components are to achieve a good separation, in determining the scope of good linearity, recoveries were between 99% ~ 101%. Conclusion The quantitative method is simple and feasible, reproducible and can be used as quality control of oral bone health. [Keywords:] bone-kang oral psoralen isopsoralen high performance liquid chromatography Abstract: ObjectiveTo establish a method of HPLC for determining psoralen and isopsoralen in Gukang Oral Liquid. MethodsThe effective components in Gukang Oral Liquid were determined by HPLC. ResultsThe resolution and the linearity were fine with the rate of recovery of psoralen 99.96%, RSD = 1.16 %; the recovery rate of isopsoralen was 100.09%, RSD = 0.60%. ConclusionThe quantitative method for determining the ingredients of Gukang Oral Liquid is simple, feasible and repeatable, and can be used for quality control of Gukang Oral Liquid. Keywords:: Gukang Oral Liquid; Psoralen; Isopsoralen; HPLC Gukang oral liquid by psoralen, Epimedium, Cistanche, white peony root, astragalus and other herbs flavor composition of 10, has kidney Zhuanggu, promoting blood circulation Tongluo, spleen Qi efficacy, patients are treated for the treatment of menopausal women, caused by osteoporosis. A total of fried Gukang oral compound is conducive to psoralen and Isopsoralen fried out [1,2], so by water extraction and alcohol precipitation was fabricated [3]. In view of psoralens, psoralen can be transformed into each other [4,2], the original criterion used by the TLCS Determination of psoralens, psoralen between the total amo