解析化学考研面试问题.docVIP

药物分析实验典型问题 鉴别检查在药品质量控制中的意义及一般杂质检查的主要项目是什么? What are the purposes of drug identification and test? What are the usual items of drug tests?. 比色比浊操作应遵循的原则是什么? What are the standard operation procedures for the clarity test? 试计算葡萄糖重金属检查中标准铅溶液的取用量。How much of the lead standard solution should be taken for the limit test for heavy metals in this experiment? 古蔡氏试砷法中所加各试剂的作用与操作注意点是什么? What precautions should be taken for the limit test for arsenic(Appendix VIII J， method 1)? And what is the function for each of the test solutions added? 根据样品取用量、杂质限量及标准砷溶液的浓度，计算标准砷溶液的取用量。Figure out the amount of the arsenic standard solution that should be taken for the limit test for arsenic(Appendix VIII J， method 1) (0.0001%) in this experiment with the specified quantity of 2.0 g of sample. 炽灼残渣测定的成败关键是什么？什么是恒重？What is the key step during the determination of residue on ignition? What does ‘ignite or dry to constant weight’ mean? 盐酸普鲁卡因的鉴别原理是什么？What are the principles of the identification of Procaine Hydrochloride. 盐酸普鲁卡因注射液中为什么要检查对氨基苯甲酸？Why is the limit of 4-aminobenzoic acid tested for Procaine Hydrochloride? 薄层色谱法检查药物中有关物质的方法通常有哪几种类型?本实验属于哪种?与其它方法有何异同点? How many kinds of the limit tests for related compounds are there? What are the differences between them? Which one is used for the limit test of 4-amino-benzoic acid in Procaine Hydrochloride Injection? 醋酸氢化可的松的鉴别原理是什么？What are the principles of the identification of hydrocortisone acetate? 甾体激素中“其它甾体”检查的意义和常用方法是什么？What are the commonly used method for and the significance of the limit test for other steroids for the steroidal drugs? 哪类甾体激素可与四氮唑蓝产生反应，是结构中的何种基团参与了反应，反应式是什么？What kind of steroidal drugs can react with the alkaline tetrazolium blue TS? What is the chemical reaction equation? 氯贝丁酯的鉴别原理是什么？What are the principles of the identification of clofibrate? 氯贝丁酯中为什么要检查对氯酚？其方法及原理是什么？Why is the limit of p-Chlorophenol tested for clofibrate? What kind of method is employed for the test and what is the principle? 气相色谱法检查杂质有哪些方法，试比较