Preparation and identification of clear resin particle method.docVIP

 PAGE \* MERGEFORMAT 9 Preparation and identification of clear resin particle method [Abstract] Objective: To establish a clear resin particles Preparation and identification methods. Methods: The prescription alcohol extraction methods using ultrasonic extraction and made into granules; using thin-layer chromatography system of the present granule Shouwu, cassia seed, and hawthorn for qualitative identification. Results: The particle preparation process is simple, thin spots clear, negative control without interference. Conclusion: The CLT particle preparation process is simple, reasonable and feasible method of identifying and reliable. [Keywords:] clear resin particles; Preparation; identification Hyperlipidemia refers to the serum total cholesterol (TC) increased, low-density lipoprotein cholesterol (LDL-C) increased, triglycerides (TG) increased, and its essence is elevated levels of serum lipoproteins, so also known as the high hyperlipoproteinemia. The role of traditional Chinese medicine in relation to lipid-lowering medicine more complicated, less toxicity. Qing lipid particles from the system Shouwu, cassia seed, hawthorn and other drugs made compatibility with Huazhuo lipid-lowering effect of Runchang catharsis for phlegm block hyperlipidemia, Zheng Jian dizziness, chest tightness, constipated. In this study, the preparation of clear resin particles, and thin-layer chromatography (TLC) of the system Shouwu, cassia seed, and hawthorn were qualitatively identified, the establishment of the granules of quality control methods. Reported as follows. An instrument and reference substance 1.1 The main instruments One ten thousandth electronic balance (U.S. PE firm); SB2200-T-type ultrasonic cleaner (Shanghai Ott Sainz Instruments); chromatography tank (10 * 10). 1.2 Reference Standards Emodin reference substance ,110756-200110; chrysophanol ,110796-200311; ursolic ,110742-200527, China’s pharmaceutical and biological products. 2 Experimental part