Red Song Songta essential oil combination of solid phase microextraction gas chromatography mass spectrometry.doc

 PAGE \* MERGEFORMAT 10 Red Song Songta essential oil combination of solid phase microextraction gas chromatography mass spectrometry Of: Meng Qi, Yang Xin, Wang Jing, Ma Ying, DING Yi [Abstract] Objective To analyze the composition of volatile components of red Songsong Ta and content, and compared three SPME fiber head of red Song Songta effect of volatile oil extraction. Methods PA, PDMS, PDMS / DVB 3种extraction Head volatile components of red Songsong Ta enrichment by GC-MS analysis of the composition of volatile components. Finally, the use of standardized values #8203;#8203;of the cumulative peak area to evaluate the sensitivity of its extraction. the results of 43 compounds extracted from PA, PDMS, and PDMS / DVB compounds in the extracts of 46 species, of which there are 28 kinds of compounds. Conclusions of volatile components of red Song Songta mainly monoterpenes and sesquiterpenes, in which higher levels of components of @ - pinene, D-limonene, β - pinene, (1S) -3,7,7 - trimethyl bicyclo [4.1.0] -3-- .3 heptene other kinds of SPME extraction of volatile components in the type and quantity are significantly different, by Extraction of volatile components in pine cone types, quantity and value of the cumulative analysis of standardized peak area compared to determine the best extraction efficiency PDMS. [Keywords:] pine; pine cone; volatile oil; solid phase micro extraction; gas chromatography mass spectrometry Abstract: ObjectiveTo analyze the composition and content of essential oil from Pine cone of Pinus koraiensis, and compared the extraction effect of three kinds of solid-phase micro-extraction fiber on essential oil from Pine cone of Pinus koraiensis. MethodsThe essential oil from Pine cone of Pinus koraiensis was extracted by PA, PDMS and PDMS / DVB-three fiber, the chemical composition was analyzed by GC-MS, and their extraction sensitivity was evaluated by cumulative area normalization value.ResultsPA extracted 43 kinds of compou