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LabGPrecipitationhardening-Directory
Precipitation hardening
Objective
The objective of this laboratory is for you to explore the kinetics and strengthening of Al by precipitation
hardening.
Preparation
Read sections 10.1‐10.5 of Meyers and Chawla.
Equipment and samples
• First week: Differential scanning calorimeters; ovens for heat treating Al alloys. Second
week: mechanical testing facilities in Talbot.
• Discs of Al 2024 alloy for DSC studies; bars of Al 2024 for tensile testing and hardness
testing.
• Computer, plotting software.
Introduction
Pure fcc metals such as Al have low yield strengths because the stress required to move a dislocation is
small. One method of strengthening an alloy is through precipitation reactions. Precipitation hardening
is the process of hardening or strengthening of an alloy by precipitating finely dispersed precipitates of
the solute in a supersaturated matrix. This process involves the following three basic steps:
1. The first step is the solution heat treatment or homogenization. Figure 1 illustrates this
phenomenon. During this step, an alloy of composition X is heated to a temperature T ,
1 1
between the solvus and solidus temperatures and soaked there until all of the solute dissolves
into the α phase and a uniform solid‐solution structure is produced.
2. The second step is quenching. Quenching is simply cooling the sample rapidly to a lower
temperature, T3, usually room temperature, and the cooling medium is usually water at room
temperature. During quenching, the solute is not immediately able to diffuse out of a phase and
the alloy is said to be supersaturated. The rationale behind the quenching process is to preserve
the uniform soli
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