HZ-202阴离子交换树脂吸附茶氨酸的研究.PDFVIP

安徽农业大学学报, 2013, 40(2): 254-257 Journal of Anhui Agricultural University 网络出版时间：2013-3-7 17:52:37 [URL] /kcms/detail/34.1162.S1752.023.html HZ-202 阴离子交换树脂吸附茶氨酸的研究 1 1 2 1* 张天明 ，谢鑫陟 ，杜守平 ，高学玲 (1. 安徽农业大学茶与食品科技学院，合肥 230036 ；2. 黄山天健农业科技有限公司，黄山 245700) 摘 要：研究了茶氨酸在一种阴离子交换树脂 HZ-202 上的动态吸附与解吸过程，确定了 HZ-202 阴离子交换 树脂吸附解吸茶氨酸的较优操作参数。结果表明，HZ-202 对茶氨酸有较好的吸附能力，动态吸附的较优参数为茶 -1 -1 氨酸浓度 1.0 mg·mL 、上样流速0.75 mL·min 、料液pH 值 6、料液温度25 ℃，吸附率超过98%；洗脱的较优参 数为洗脱剂 NaOH 浓度为 0.02 mol·L-1 、洗脱速度0.75 mL·min-1 下，解吸率为 86.22%。 关键词：茶氨酸；HZ-202 阴离子交换树脂；吸附；洗脱 中图分类号：TS272; O647.3 文献标识码：A 文章编号：1672−352X (2013)02−0254−04 Preliminary study on adsorption of L-theanine with anion exchange resin HZ-202 1 1 2 1 ZHANG Tian-ming , XIE Xin-zhi , DU Shou-ping , GAO Xue-ling (1. School of Tea Food Science and Technology, Anhui Agricultural University, Hefei 230036; 2. Huangshan Tianjian Agricultural Sci-Tech Ltd., Huangshan 245700) Abstract: The adsorption and desorption behaviors of L-theanine with HZ-202 anion exchange resin were investigated. The dynamic kinetics of HZ-202 anion exchange resin was studied, and the optimum parameters of adsorption were procured. It was shown that the pH value and concentration of L-theanine, the flow rate and tem- perature affected the kinetic curves of HZ-202 anion exchange resin to L-theanine. The optimum adsorption con- ditions were the flow rate 0.75 mL·min-1, sample concentration 1.0 mg·mL-1, pH 6, and temperature 25℃；And the -1 -1 optimum desorption condition