含铟铅烟尘提铟试验研究.pdfVIP

34 3 稀 有 金 属 2010 5 Vol34 No3 CH INESE JOURNAL OF RARE METALS May 2010 * 高照国 , 曹耀华, 刘红召 ( 中国地质科学院郑州矿产综合利用研究所, 国家 金属矿资源综合利用工程技术研究中心, 河南郑州450006) : , P204 , 200 gL- 1 1. 25% 95 5 h 2 h 91. 5% ; P204 15% , O /A= 1/15, 5m in 9 % ; 6N , 100% ; , 99. 7% : ; ; ; do:i 10. 3969/.j issn. 025 - 7076. 2010. 03. 01 : TF 43 : A : 025 - 7076( 2010) 03- 0413- 07 I ndium E xtraction Process from Lead Soot w ith I ndium * Gao Zhaoguo , CaoYaohua, L iu H ongzhao (Zhengzhou Institute of Multipurpose Utilization of M ineralResources, ChinaA cademy of Geolog icalSciences, China N ational ngineering Research Centerf or Utilization of IndustrialM inerals, Zhengzhou 450006, China) Abstract: A ccording to the characteristics and properties of lead sootw ith ind ium, an indium extraction processw ith tw o stage vitriol leach ing, P204 extraction, sulfuric acid wash ing, hydroch loric acid reverse extraction, replacing indium by zinc powder w as estab - 1 lished. Results show ed that the leach ing rate was 91. 5% when the original acidity was 200 gL , the quantity of oxidan tw as 1. 25, the leach ing tem peraturew as 95 , the concentrated acid leach ing tmi ew as 5 h, the d ilute acid leach ing tmi e was 2 h. Indium extrac tion rate was 9 % w hen the concentration of P204 was 15% , O /A w as 1/ 15 and extraction tmi e w as 5 m in. The backextraction rate w as 100% w hen 6N H C lwas used as backextract and three step reverse reextractionw as adopted. Ind ium in the reextracted solu tion w as replaced by zinc power and the replacem ent ratew as m ore than 99. 7% . K ey word s: lead soot; indium extraction; leach ing; extraction ( In), , - 5