抗坏血酸棕榈酸酯测定方法的比较.pdfVIP

质量安全 粮油食日科技第22 卷 2014 茸第3 期 抗坏血酸棕榈酸醋测定方法的比较 杜淑霞，司徒满泉，徐丽，滕晓焕 (广东轻工职业技术学院食品与生物工程系，广东广州 510300) 摘 要:将改进滴定琪法应用于抗坏血酸棕榈酸醋含量的测定，并与棋滴定法和硅钮兰分光光度法 进行了比较。结果表明，几种常用方法的测定结果略有差异，{食品添加剂手册》中的棋滴定法由 于溶液混浊影响终点判断，导致结果偏高，重现性较差;硅钳兰分光光度法灵敏度较高，但需要试剂 多，测定周期长;滴定琪法与 GB 16314 -1996 中方法的测定结果在5% 水平上无显著差异，但由于 滴定琪法中淀粉指示剂变色更明显，易于判断滴定终点，方法的精密度更高，且简单快速，可用于抗 坏血酸棕榈酸醋含量的日常检测。 关键词:L- 抗坏血酸棕榈酸醋;测定方法;比较 中图分类号:TS 202.3 文献标识码:A 文章编号: 1007 - 7561 (2014) 03 - 0064 - 03 Comparison of the determination methods of ascorbyl palmitate DU Shu - xia , SITU Man - qu剧，XU Li ,TENG Xiao - huan (Department of Food and Bioengineering ,Guangdong Light Industry Vocational and Technical College ,Guangzhou Guangdong 510300 ) Abstract: The ascorbyl palmitate was determined by the improved iodimetIγand compared wi由 iodimetry and silicon molybdenum blue spectrophotometer method. The results showed that there were slight differ- ences among the results determined by the common methods. The result by the iodimetry according to Food Additive Manual was leaning high and poor repeatability because of the turbid solution; the result by silicon molybdenum blue spectrophotometer method has a higher sensitivity , but needs more reagents and longer determination period. No significant difference between the results in GB 16314 -1996 and iodom- et巧 at 5 % level. The improved iodometry w副 easier to judge the end point of titration and had a higher precision , since the color change of the starch indicator was more obvious. This method is easy and quick , and can be used for the daily determination of the ascorbyl palmitate. Key words: L - ascorbyl palmitate; determination methods; comparison 抗坏血酸棕