粉末注射成形TiAl超固相线液相烧结工艺研究.pdfVIP

维普资讯 学兔兔 第26卷第2期 粉末冶金技术 Vo1．26，No．2 2008年4月 Powder Metallurgy Technology Apr．2008 粉末注射成形TiA1超固相线液相烧结工艺研究* 赵丽明 )一 曲选辉 李世琼2 何新波 1)(北京科技大学材料科学与q-程学院，北京 100083) 2)(钢铁研究总院，北京 100081) 摘 要： 以Ti一47．5％ 一2．5％V一1．0％Cr(原子数分数)气雾化预合金粉末为原料，采用粉末注射成形 工艺制备了TiA1合金材料，重点研究了该TiA1合金超固相线液相烧结温度区间和保温时间以及烧结体显微 组织、密度和压缩性能的变化规律。结果表明：烧结温度在 1 410～1 450℃，保温时间在 1h以内，烧结体可以 致密化；在1 450℃保温30min，烧结体相对密度可以达到95％，烧结体的抗压强度为2 105MPa，压缩率达到 30．9％，接近铸态合金力学性能；随烧结温度升高，烧结体近片层组织中的7等轴晶逐渐减少，片层团逐渐增 加。 关键词：钛铝合金；气雾化钛铝粉末；粉末注射成形；超固相线烧结 Supersolidus liquid phase sintering process for inj ection molded TiA! Zhao Liming”， Qu Xuanhui¨，Li Shiqiong2)，He Xinbo ) 1)(School 0f Material Science and Engineering，University of Science and Technology Beijing，Beijing 100083，China) 2)(Central IronSteel Research Institute，BeJjing 100081，China) Abstract：This paper is dealing with an injection molding of gas atomized pre—alloy powders of Ti一47．5AI一2．5V一 1．0Cr．The sintering temperature range，sintering time and the effects of sintering temperature on microstructure， density and compressive property of the alloy of supersolidus liquid phase sintering were investigated．Results Show that the specimens can be densified rapidly at 1 410—1 450℃ for 60 min．When vacuum sintering is employed．a near ful1 density of 95％ is obtained at 1 450℃ after 30 min holding．the compression strength and compression ratio are 2 105MPa and 30．9％ respectively．which is close to that of cast alloy．With sintering temperature increasing，the amount of 7 phase decreases gradually and the amount of lamellar phase increases guadually．