微波辅助萃取当归精油的条件优化研究.pdfVIP

微波辅助萃取当归精油的条件优化研究 Microwave-assisted extraction of essential oils from angelica sinensis 邓湘庆1 龚盛昭2 DENG Xiang-qing1 GONG Sheng-zhao2 （1. 广东食品药品职业学院化妆品系，广东 广州 510520；2. 广东轻工职业技术学院轻化 工程系，广东 广州510300） （1.DepartmentofCosmetics,GuangdongFoodandDrugVocationalCollege,Guangzhou， Guangdong 510520,China；2. Department of Chemical Engineering, Guangdong Industry Technical College, Guangzhou，Guangdong 510300，China） 摘要：应用单因素试验和正交试验，考察提取剂类型、微波功率、微波辐射时间、液料质量 比、液料湿度和物料粒度对提取效果的影响，得到微波辅助提取香附精油的最佳条件：以石 油醚为溶剂，微波功率450 W，萃取2次，每次120 s，每次用液料质量比为8 ∶1。萃取液 进行真空浓缩至无溶剂蒸出，得精油粗产品。往精油粗产品中加入乙醇溶解，放入－15 ℃冰 箱中冷冻48 h，离心分离去除树脂状物质，过滤，滤液进行真空浓缩后，即得当归精油，产 率约3.4%，纯度96.1 %。 关键词: 精油；当归；微波辅助提取 Abstract:The effects of extraction variables, especially solvent type, microwave power, the microwave irradiation time, materials-solvent mass ratio, moisture content and particle size of materials on extraction efficiency were investigated using single factor test and orthogonal method. The optimum conditions are obtained: Petroleum ether as solvent, extracting twice, microwave power 450 W, irradiation time 120 s, solvent-material mass ratio 8 ∶1. The extracted solution was concentrated under vacuum to give crude essential oil which was dissolved in ethanol and frozen at –15 ℃ for 48 h. The solution was then separated centrifugally and filtered to get rid of impurities. The essential oilwith yield of 3. 4 % and purity of 96.1 % was then obtained after distilling the liquor under vacuum. Keywords: Essential oils； Angelica sinensis；Microwave-assisted extraction ———————————— 1 作者简介：邓湘庆 （1964－），男，广东食品药品职业学院化妆品系工程师。 E-mail: dxq888@vip.sohu.net 收稿日期：2007-06-11 微波萃取技术是种新型萃取技术，具有生产率高、纯度高，速度快、物耗能耗低、环保等 优点。可显著降低成本，而且质地更均匀，克服传统萃取技术产品质量难以控制，疗效不稳 [1,2] 定，实验结果重现性差等缺陷，大大减少