灰化蒸馏_氟试剂比色法与离子色谱法测定茶叶中氟含量的比较.pdfVIP

2010 6 16 6 Pr v M d Trib, Vol . 16, No. 6, J un. 2010 549 - 高素虹, 蔡梦华, 洪祥奇 ( 汕头市疾病预防控制中心, 广东 汕头 515031) : R 1555 : B : 1672- 9153( 2010) 06- 0549- 02 : [ 目的] -, [ 方法] , -, t [ 结果] -408% ~ 839% , 214% ~ 495% , ( t t ( 005, 14) , P 005) [ 结论] -, , : ; ; ; - Comparison on Determination of the Content of Fluoride in Tea with Cineration Distillation- color Method of Fluorine Re- agent and Ion Chromatography/ GA O S u-hong, CA I M eng-hua, H ON G X iang-qi(S hantou Center f or D isease Contr ol and Pr ev ention, Shantou 515031, China Abstract: Objective] T o com par th advant ag s and disadvantag s of cin ration distillation-color m thod of fluorin r ag nt and ion chromatography, choos th b tt r d t rmination of fluorid in t a Methods] Th sampl w as solid fluo- rin , imm rsion, carbonization and cin ration, by cin rat ion distillat ion-color m thod of fluorin r ag nt and ion chroma- tography w r m asur d, th pr cision and accuracy was compar d with t xamination Results] T h RSD valu w as 214%-495% by ion chromatographic d t rmination of fluorid in t a, th RSD valu w as 408%- 839% by cin ration distillation-color m thod of fluorin r ag nt, aft r th t t st, t t ( 005, 14) , P 005, w ith no statist ical signif icanc Con- clusion] Ion chromat ographic d t rminat ion of fluorid in t a wit h high pr cision and accuracy, t h op rat ion is sim pl , rap- id, and so is suitabl for larg quantit i s of sampl s Key words:T a l av s; Fluorid ; Ion chromatography; Color m thod , , , , , , , 1 , , 11 主要 器与试剂 U V-540 [ 2