压力对Zn-22Al合金晶体结构及微观组织的影响.pdfVIP

学兔兔 Jun．2011 V0I．6O N0．6 -～● -^ 、’ 、● -^● - _^ — ^ ；新材料·新T艺 { ， ’●■ ■l^ ’r●^，■’■，帅 _、 ■ 压力对Zn一22AI合金晶体结构及微观组织的影响 包艳青 ，袁朝圣 ，白彦华 ，t李荣德 (1．沈阳工业大学材料科学与工程学院，辽宁沈阳110870；2．西南交通大学高温高压物理研究所，四川成都610031) 摘要：研究了高压条件下凝固和常压凝固的Zn一22A1合金的晶体结构和显微组织。所采用设备与通常研究压力凝固的 设备不同，可实现快速增压，即2Oms内能加压至5．5GPa。扫描电子显微镜观察其组织形貌的变化，不同压力下，组织 形态发生显著变化，由常压下的树枝晶状过渡为3GPa下的网格状，且后者的组织明显细小致密均匀。利用x光衍射仪 对试样的相组成分析和晶格常数的计算，发现压力改变了试样的晶格常数。 关键词：Zn．Al合金；显微组织；高压；晶格常数 中图分类号：TG146．2 文献标识码：A 文章编号：1001—4977(201 1)06—0533—03 Effect of Pressure on CrystaI Structure and Microstructure of Zn．22AI Al loy BAO Yan—qing ，YUAN Chao—sheng ，BAI Yan—hua’，LI Rong—de’ (1。School of Materials Science and Engineering，Shenyang University of Technology， Shenyang 1 1 0870，Liaoning，China；2．Laboratory of High Pressure Physics， Southwest Jiaotong University，Chengdu 61 0031，Sichuan，China) Abstract：Specimens with different pressure were produced by rapidly compression process，and the effect of pressure on the crystaI structure and microstructure of Zn-22AI alloy were studied．The equipment used jn this study features fast pressurization that the melted sample can be pressurized tO 5．5 GPa within 20 ms．The microstructures of the obtained samples were characterized by scanning electronic microscopy．The results show that the morphology and microstructure alters obviously with the pressure．The morphology of the alloys changed frOm coarse dendrite under normal pressure to fine latticework under 3 GPa．and the structure of 3 GPa specimen iS remarkably smaller than that of normaI pressure specimen．Besides．the remarkable change of Iattice constant