三溢流分隔壁塔板上气含率的研究-学兔兔 www.xuetutu.com.pdfVIP

学兔兔 石 油 化 工 · 646· PETR0CHEMICAL TECHN0L0GY 2013年第42卷第6期 三溢流分隔壁塔板上气含率的研究 郑瑞朋，齐 亮，田端正，姚克俭 (绿色化学合成技术国家重点实验室培育基地 浙江工业大学 化学工程与材料学院，浙江 杭州 310032) [摘要]在内径为1 200 mm实验塔中，以空气和水为实验介质，采用电导率法对三溢流分隔壁塔板上的气含率进行了测定， 并探讨了塔板上气含率分布的规律。实验结果表明，当塔板上高度低于60 mm时，三溢流分隔壁塔板上小鼓泡区内的面平均 气含率比大鼓泡区内的大；当板上高度高于60 mm时，小鼓泡区内的面平均气含率比大鼓泡区内的小；在塔板上35 mm处(气 含率的最低测量点)，小鼓泡区和大鼓泡区内的气含率分布不均匀性指数的差值最大，随板上高度的增加，该差值逐渐变小 并趋于零；在塔板上高度低行125 mlTl处，平面壁面鼓泡区的壁面效应较曲面壁面鼓泡区要弱，板上高度高于125 mm后，不同 鼓泡区的气含率分布不均匀性指数的差值趋于零。 [关键词]三溢流分隔壁塔板；气含率；电导率法；鼓泡区 [文章编号]1000—8144(2013)06—0646—05 [中图分类号]TQ 053．5 [文献标志码]A Study on Gas Hold--up Fraction on Three--Pass Dividing Wall Tray Zheng Ruipeng，Qi Liang，Tian Duanzheng，Yao Kejian (State Key Laboratory Breeding Base ofGreen Chemistry—Synthesis Technology，College ofChemical Engineering and Materials Science，Zhejiang University ofTechnology，Hangzhou Zhejiang 310032，China) [Abstract J Gas hold—up fraction on three—pass dividing wall tray with air and water as media was measured in an organic glass column with inner diameter 1 200 mm by means of conductometry．The distribution of the gas hold—up fraction on the tray floor was investigated．The experimental results show that。when the height from tray floor is less than 60 mm．the average gas hold—up fraction in small bubbling area on the three—pass dividing wall tray is higher than that in big bubbling area， and when the height from tray floor is more than 60 mm，the average gas hold-up fraction in small bubbling area is lower than that in big bubbling are