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化学需氧量常用测定方法的比拟(国外英文资料)
化学需氧量常用测定方法的比较(国外英文资料)
The comparison of the method of chemical oxygen demand is commonly measured
Shanshan came to hefei han jia zhen
(Beijing municipal environmental monitoring station, Beijing 100035)
Abstract: compared with the national standard method for determination of chemical oxygen demand (cod), rapid determination method, the advantages and disadvantages of air-cooled digestion method and coulomb method, for rational selection of the appropriate monitoring method provides a theoretical basis.
Keywords: COD, potassium bichromate, determination, oxidation reduction
Chemical oxygen demand (CODcr) is one of Chinas implementation of total discharge control indicators, it reflects the degree of water polluted by reducing agents, the water reducing agents include organic matter, nitrite, ferrous salt, sulphur, etc. It is also common for water samples to be contaminated by organic matter, so chemical oxygen demand is also a measure of the relative content of organic matter. The chemical oxygen demand (cod) values of water samples from kinds and concentrations of oxidizing agent, acidity of reaction solution, reaction temperature and time, and in the presence of catalyst and obtain different results, is a conditional indicator, in our country for the determination of wastewater with potassium dichromate method, such as using other methods, must do the control experiment with potassium dichromate method, below I will put in several measuring method commonly used in the lab for comparison:
The CODcr was determined by a chemical method
1.1.1 dichromate method GB/t11914-89
Potassium dichromate method is a classic of the laboratory analysis method, is also a national standard method, usually used with other methods at experiment, potassium dichromate method using water samples in strongly acidic solution oxidative reflux 2 hours of pretreatment, oxidation so as to make the most of the organic matter in water samples was completely, has a wide measuring range (5-700 m
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