Waters液相层析问题排除(英)-1.pptVIP

* * Parallel flow path. 515 drawoff valve is on outlet side of pump, 510/600 on inlet side. * Cut away view of the 2690 / 2695 showing the location of various assemblies. * FIFO - First in, first out results in mixing in heads. Gradients run smoothly. * 1. Serial Flow Path – Solvent blending in piston chambers 2. Independent Piston Drive – Dual drive motors 3. Dual Pressure Transducers – Two point performance monitoring 4. Variable Piston Volume – Balanced with flow rate 5. Gradient Proportioning Valve – Low volume design * As in slide. Variable loop filling. Due to lamellar flow, need min 5X loop volume to completely fill. * Waters 717plus Autosampler Training Guide Version 2.0 * Green Teflon tubing for needle wash inlet (1/16 inch) Yellow Teflon tubing for needle wash waste (1/16 inch) Clear Teflon tubing for sample loop waste (V3) (1/16 inch) Blue stainless steel autosampler inlet from pump (.040inch) Red stainless steel autosampler outlet to system (.009 inch) Caution: Always use safe laboratory practices when handling solvents. Refer to the Material Safety Data Sheet (MSDS) for the solvents in use. * All 717+’s built after March 1995, serial number MX5BM8522M and higher, have a solenoid valve for V3. The injector motor is also shorter, this does not affect the operation of the injector. * * The normal valve configuration is Valve 1 (inject) open, Valve 2 (syringe) closed, Valve 3 (vent) closed, Valve 4 (Needle Wash) closed. Because of the restrictor loop the flow splits 95% flows through the sample loop, 5% flows through the restrictor loop. * 100% flow At the injection start, Valve 1 (V1) closes, all flow now passes through the restrictor. The needle lowers till the port is in the lower seal. Valve 3 (V3) opens, Valve 2 (V2) opens venting the pressure in the sample loop. V3 closes to prevent siphoning. The needle wash pump starts. Valve 4 (V4) opens. * With V3 closed, the needle lowers into the vial. V4