剖析常用含量计算公式(国外英文资料).docVIP

分析常用含量计算公式(国外英文资料) 55 ℃ water bath heating in 30 minutes, after cooling, the new system of 0.5 mL, 5% amino sulfonic acid ammonium solution with anhydrous ethanol diluted to scale, shake well. Another reference substance solution with 5 ml of test sample solution, besides do not add 0.3% solution of sodium nitrite, respectively in the same way as their corresponding blank after processing, according to the spectrophotometric method, were determined in 390 + 2 nm wavelengths in the absorbance, the absorbance of test sample solution is 0.604, the absorbance of the reference substance solution is 0.594, calculate the percentage content of reserpine. The calculation of the content of the tablets (1) titration analysis Direct titration: Residual titration Example: department of barbital sodium capsule (labeled amount to 0.1 g) 20 grains, measured after removing capsule contents total weight is 3.0780 g, called 0.1536 g, with bromine amount as stipulated in the pharmacopoeia method. Add the bromine (0.1 molar) 25mL, and the remaining bromine will be titrated to the end of the finish line with a sodium thiosulfite (0.1025 molar) for 17.94 mL. The blank test was used to make 25.00 mL of sodium sulphate. The percentage of the encapsulation in the capsule is calculated according to the amount of the amount indicated in the capsule, which is 13.01 mg per unit of bromo (0.1 mol/L). (2) ultraviolet spectrophotometry The coefficient of absorption (2) control method The calculation of the measured results of the injection (1) titration analysis Direct titration: Vs - volume of the product (mL) Example: vitamin C injection (0.1 g) specifications 2 mL: the content of measurement: precision measuring the product 2 mL, 15 mL and 2 mL of acetone and water, shake well, placed for 5 minutes, add 4 mL dilute acetic acid and starch indicating liquid 1 mL, with fluid (0.1003 mol/L) iodine titration titration, to show blue solution and lasts 30 seconds does not fade, consumes 10.56 mL. Ever