泡沫吸附法测定金(国外英文资料).docVIP

泡沫吸附法测定金(国外英文资料) B means the element that is measured. M - the mass of the element (component), mu g (work curve), is measured from the working curve (visual ratio of color to standard) Drawing of a blank test solution, which is applied to the measuring elements of different mass concentrations, in the coordinate paper On the top, the polarographic method draws the i-rho B curve; The absorbance is the a-rho B curve; The ion is going to choose the polar method in the semilog In the actual work, the volume and drawing of the sample solution are measured The volume of the standard solution of the working curve is consistent, so it can be found directly from the work curve The quality of mu g); Ms - call the mass of the sample, g. Five, notice the matter (1) the acid degree of adsorption Au is the best in foamed plastic, and in summer the acidity of the water is (15-85). Winter is for (20 + 80) advisable. (2) the TMK ethanol solution is kept in the shade. If the lower levels are not visible, the TMK solution must be reformulated. (3) room temperature is too high, 0 ~ 0.06 mu gAu color order fade. Foam plastic enrichment method determination gold A method feed Sample after 650 ℃ calcination, aqua regia after aqua regia decomposition (1 + 9) using foam enrichment medium by thiourea solution Au free Au (1) or ashing bubble with molding into HCl solution method (2). The test solution inhaled air - acetylene flame, use AAS method for determining the absorbance of Au, this law shall be applicable to the rock and mineral in the omega (Au) / 10-6 = 0.1 ~ 200. Second, the preparation of reagents Gold standard storage solution: the gold method is determined according to the activated carbon enrichment method. Au has a mass concentration of 1000 mu g/mL. Gold standard solution: remove 25.0 mLAu standard storage solution in 500mL volumetric flask, add 50mL of water, dilute with water to scale and mix well. This solution contains 50.0 mu g/mLAu. Instruments and working conditions W