多晶纯铝晶内局部变形组织分析.pdfVIP

重庆大学学报 Vo l. 31 No.9 第 31 卷第 9 期 2008 年 9 月 Journal of Chongqing University Sep. 2008 文章编号: 1000-582X(2008) 09-1023-05 多晶纯锦晶内局部变形组织分析 周正，冯毅，萧梅，张喜燕 (重庆大学材料科学与工程学院，重庆 400030) 摘 要:用显微硬度方法在晶拉尺度范圈内对多晶纯铭进行了晶内塑性变形，研究了返火前后 压痕周边变形组织形貌。实验发现，仅在退火后的压痕周边出现了不同形态的滑移带，在滑移带的 区域发现有大量位错露头并在某些局部范围内呈有序排列状态的现象，同时观察到滑移带直接穿 越晶内偏聚区界的现象。文中分析了没有在晶内压痕周边区域内发现再结晶现象的原因，讨论了 退火温度及时间、压下量及晶位取向等因素对滑移带形成的影响。研究表明，与整体变形方式不 同，晶内变形方法可以更方便地研究多晶材料塑性变形及再给晶时的一些组织特点。 关键词:晶粒$变形z 滑移带:纯铭:再给晶 中图分类号:TG146 文献标志码:A The structure of local transgranular deforrnation in polycrystalline pure aluminium ZHOU Zheng , FENG Yi ,XIAO Mei , ZHANG Xi-yan (College of Materials Science and Engineering , Chongqing University , Chongqing 400030 , P. R. China) Abstract: The micro-hardness method was used to achieve plastic deformation in grain scales in polycrystalline. pure aluminums. Characteristics of the deformation structure near indentations were investigated before and after annealing. The different morphologies of slipbands near indentation areas were viewed only after annealing. Within the slipband areas the numerous orderly arranged ends of the dislocations were identified. During experiments , we observed the phenomenon of slipbands across aggregate areas in grains. We discuss reasons for not discovering recrystallization in the deformed specimen after annealing. We also discuss factors such as temperature and time of annealing , reduction and grain orientation , which have influence on the formation of slipbands. The experimental results show that , being different from global deformation for materials , the mode of transgranular deformation