X射线荧光元素分析技术快速测定化妆品中的吡硫嗡锌.pdfVIP

重辞斗琶稿(剧姐 :Ð15 f王 12 月第6 期 f1AVOUR~R岛、CEαE画面mcs 1)凹企胃，2015 ，NO. 6 X 射线荧光元素分析技术快速测定化妆品中的毗硫嗡铸铃 .. 作者简介 陈、张好(1981一) 1 女， 硕士， 主管药师. 广东省食品药品检验F斤，广东广州 5HJt 80 主妥从事化妆品检测分析研究。 · 陈张好用智明刘小娟张弦 联系也话:020 E -mail: hoeyl017@163.com 采用适用于化妆品基质检测的模式. 应用 X 射线荧光元素分析技术(XRF) 快速测定样品中的 Zn 元素，并计算去屑类化 枚品中毗硫嗡锦含量e 方法:X 射线荧光元素分析仪.测试时间 120 ~，标准偏差 2(]，采用模式;化技品模式。 结果:Zn 元素在 100-3 SKI mg/kg 之间呈良好线性关系。力目标回收率 97.7%-101. 3%. 检出质量比为 10 mg/kg. 结论g 该方法简便快速、 准确度高.i吁用于tk速测定化妆品中的口比硫l嗡镑。 g盟E X 射线荧光化妆品毗毓嗡镑快速测定 Rapid Determination of Pyrithione Zinc in C os metics b y X-Ray FJuorescence Elemental Analysis Technology锺 CHEN ZhU11ghuo ZHOU Zhiming LlU Xiaojuu r/ ZHANG Xian (Guangdong I n~titute for Food and Drug Control , Guangzhou 510180 , Guangdong , Ch ina) Abstract: To 归tablish a method for rapid determination of pyrithione zinc in cosmetics. the X-ray fluorescence elemental technology with a appropriate model was applied. in which. X-ray fluorescence elemental analyzer was used . test time was 120 s . standard deviation was .2 (]. and cosmetic mode was used. The results showed that the linear range~ were in 100 to 3 500 mg/ kg for Zn. The average recovcrics were between 97. 7% and 101.3%. The detectìon limit was 10 mg/ kg for Zn. The mcthod is simple. rapid and accurate. it can be u~ed for the rapid detennination 01 pyrithione zÎnc În cosmetics. Key 附rds: X-ray fluorc!cence cosmetics pyrithione zinc rapid detennination 1 材料与万法 毗硫嗡辞(简称 ZPT)是目前公认有效且使用