气相色谱法测定活络膏中薄荷脑和水杨酸甲酯的含量论文.docVIP

　　气相色谱法测定活络膏中薄荷脑和水杨酸甲酯的含量论文 .freel×0.25 mm×0.25 μm,程序升温,起始温度为80℃,保持5 min后每分钟升高15℃,终止温度为190℃,保持8 min,分流比50∶1。结果:各组分在相应的浓度呈良好线性关系,r1=0.999 79、r2=0.999 98,RSD≤2.0%。结论:本方法简便、快速、准确,可用于活络膏的质量控制。 关键词 活络膏;薄荷脑;水杨酸甲酯 Determination of the contents of mentholum and methyl salicylate in Medicated Balm by capillary gas chromatography MO Huodi, RONG Lingxin, HE edicated Balm by capillary gas chromatography. Methods: Chromatographic condition n 30 m×0.25 mm×0.25 μm, initial temperature perature programmed to raise 15℃ in five minutes, final temperature inutes, split ratio ethod is sensitive, accurate