响应面优化超临界CO2萃取八月瓜幼果多酚工艺.pdfVIP

76 2015, VoJ. 36, NO.10 自自融事 ※王艺技术 萃取八月瓜幼果多盼王艺 响应面优化超i临界CO 2 顾仁勇，杨万根，余估 (吉首大学化学化工学院，湖南吉首 416∞0) 摘 要z 为了综合利用八月瓜幼果资源，采用超临界CO 萃取技术提取八月瓜多盼。探讨了不同体积分数乙醇溶液 2 作为夹带剂对多盼的萃取效果，采用响应面法，以多盼萃取得率为响应值，考察原料与夹带剂的料液比、萃取压 力和萃取温度对多酣萃取的影响，并优化萃取条件。结果表明:以体积分数95%乙醇溶液为夹带剂，可使八月瓜 幼果多盼萃取得率提高约2.45 倍，产品纯度提高约15.49%; 优化所得最佳条件为料液比1 :2.6 (g/mL)、萃取压力 37MPa、萃取温度51 OC ，此条件下八月瓜幼果多盼萃取得率可达6.4 1%，产品纯度为87.69%0 关键词:八月瓜幼果:多盼:超临界CO 萃取:夹带剂:响应面优化法 2 Optimization of Supercritical CO2 Extraction Conditions of Polyphenols 仕om Young Pruits of Holboellio lat价lia by Response Surface Methodology GU Renyong , YANG Wangen , YU Ji (College of Chemistry and Chemical Engineering, Jishou University , Jishou 416000 , China) Abstract: Polyphenols were extracted from the young fruits of Holboellio latifolia by supercritical CO2 extraction. The effect of ethanol concentration on extraction efficiency was examined. The extraction conditions solid/liquid ratio (namely materiaUentrainer ratio) , extraction press町e and temperature were investigated and the optimum extraction conditions were obtained by response surface methodology. The results showed that the extraction yield and purity of polyphenoIs were enhanced by 2 .45 times and 15.49%, respectively , when using 95% ethanol as the entrainer, in comparison to those obtained without the entrainer. The optimum extraction conditions for solid/liquid r