“二元液系相图”实验的综合改革研究.pdfVIP

· 98· 实验科学与技术 2007年l2月 “二元液系相图实验的综合改革研究一。 向明礼 ” ，曾小平 ，滕奇志 ，王旭阳 ，陈建钧 (1．四川大学化工学院，成都 610065；2．绵阳师范学院物理与电子信息工程系，~t)Jl绵阳 621000) 摘要：对物理化学实验中“二元液系相图”实验项目，从改进实验装置、提升实验手段，改善实验教学方法等方面，进行了 综合改革研究。研究结果在实验教学中的应用表明，从新旧装置所获得的实验结果，对比显著；基于Windows操作平台的 数据处理软件能在一定温度范围内的任意温度下，消除阿贝折光仪的读数漂移，迅速、准确地获取二元液系汽一液相平衡 组成，帮助教学双方通过观察图形及时对实验结果进行判断，及时发现问题、分析问题和解决问题。采用改善的教学方法， 没有相应物理化学背景知识的一年级工科化学学生，也能取得好的实验结果。 关 键 词：物理化学；相图；实验装置；二元液系；软件 中图分类号：G642·423 文献标识码：B 文章编号：1672～4550(2007)06～0098—03 On Educational Reform of Physicochemical Experiment of Two—component Liquid State Phase Diagram’’ XIANG Ming—lj ，ZENG Xiao—ping ，TENG Qi—zhi ，WANG Xu—yang ，CHEN Jian-jun (1．Chemical Engineering College．Siehuan University，Chengdu 610065，China； 2．Mianyang Teachers College，Oelmtme．t of Physics and Electronic Information Engineering，Mianyang 621000，China) Abstract：The physicochemical experiment of Two—component厶gu State Phase D is comprehensively studied from three鹪- peets：improving experimental facility，bettering means of data processing and reforming experimental methods．The results of studies have been applied to experiment teaching．Results show that the improved experimental facility is much better than the old one in pre- cisoly obtaining experimental data．The data—processing software based on Windows system is programmed by the project team here in- dependently．It is qnite strong in getting constituting data from working culwe due to its ability to calibrate a variety of deviations．It helps both teachers and students discover，analyze and solve problems． Freshmen who lack relevant physicochemical knowledge also n satisfactory experimental results with reformed educational methods． Key words：physical chemistry；phase diagram；experimental facility；two—component liquid state；software