16617 cas ：120-47-8 对羟基苯甲酸乙酯.pptVIP

HOT NEWS 沐浴乳 含有『Paraben』防腐劑，超過10年就可能誘發乳癌。那保養品呢？塗在皮膚上滲透吸收不是更慘 /watch?v=IyiKM6Z-Rp0 2011/04/11 黃俊強 INTRODUCTION Parabens are stable in air, and resistant to hydrolysis in hot and cold water and in acidic solutions (up to pH 7). Parabens are used in pharmaceutical and cosmetic products because of their broad spectrum of activity. Studies on the determination of parabens in human breast cancer cells. Analytical-grade borax, acetonitrile, methanol,and sodium hydroxide were provided by Merck. Apparatus Apparatus Apparatus Fused-silica capillary total and effective lengths of 75 and 50 cm (Unimicro) pH 301 pH/ion meter(Hanna Instruments, Sarmeola di Rubano, Italy). Supelclean LC-18 (Supelco Inc., Beilefonte, PA, United States) High-quality water was obtained using a model of Water Pro PS Labconco Corp. (Kansan City, Missouri). Standard and sample solutions RESULTS AND DISCUSSION CONCLUSIONS A simple, fast, efficient, cheap, and reliable CE method has been developed and validated for the analysis of methyl, ethyl, propyl, and butyl parabens. The method offers advantages such as a short analysis time, a low LOD, LOQ, and reagent consumption. It provides an alternative procedure for the quality control of parabens in pharmaceutical and cosmetic products. Summary 2008年U. D. Uysal團隊開發CZE結合SPE前處理方法能在12分鐘內偵測出牙膏、洗髮精、糖漿、染髮劑中的對羥基苯甲酸酯類(甲酯、乙酯、丙酯、丁酯)，其最佳化條件為緩衝溶液20mM borate pH 9，樣品中添加甲醇溶劑10%，電壓設定為20kV，波長為200 nm， 其LOD值1.42~2.86 × 10-6 ，R值大於0.9990，並使用LC-18 solid-phase 管柱萃取真實樣品，此方法具有良好的靈敏度以及再現性，而且分析時間短，可以有效偵測市面上的產品。 * * Impact factor:0.662 * INTRODUCTION MATERIALS AND METHODS RESULTS AND DISCUSSION CONCLUSIONS * INTRODUCTION MATERIALS AND METHODS RESULTS AND DISCUSSION CONCLUSIONS 2.1 Chemicals 2.2 Apparatus 2.3 Electrophoretic Procedures 2.4 Sample and Sample Treatment 分子式：C8H8O3 分子量：152.15 CAS ：99-76-3 對羥基苯甲酸甲酯 (Methylparaben ) 分子式：C9H10O3 分子量：166.17 CAS ：120-47-8 對羥基苯甲酸乙酯 (ethylparaben) 分子式：C10H12O3 分子量：180.2 CAS ：94-13-3 對羥基苯甲酸丙酯 (propylparaben