药学 英语 附录.ppt

附录选读 * Determination of Loss on Drying Paper Chromatography Appendix IX D. Determination of Loss on Drying （测定法） (干燥失重) ( Ph. Eur. method 2.2.32 ) Loss on drying is the loss of weight expressed as % w/w. Method Place the prescribed quantity of the substance being examined in a weighing bottle previously dried under the conditions prescribed for the substance being examined. prescribed quantity 规定的量 being examined 待检的 weighing bottle 称量瓶 Place the prescribed quantity of the substance being examined in a weighing bottle previously dried under the conditions prescribed for the substance being examined. 照各药品项下规定的条件 Dry the substance to constant weight or for the prescribed time by one of the following procedures. constant weight 恒重 prescribed time 规定的时间 (a) In a desiccator The drying is carried out over phosphorus pentoxide at atmospheric pressure and at room temperature. Desiccator 干燥器 phosphorus pentoxide 五氧化二磷 atmospheric pressure 大气压 (b) In vacuo The drying is carried out over phosphorus pentoxide at a pressure of 1.5 to 2.5 kPa at room temperature. (c) In vacuo within a specified temperature range The drying is carried out over phosphorus pentoxide at a pressure of 1.5 to 2.5 kPa within the temperature range specified in the monograph. (d) In an oven within a specified temperature range . The drying is carried out in an oven within the temperature range specified in the monograph specified 指定的 oven 烘箱 (e) Under high vacuum. The drying is carried out over phosphorus pentoxide at a pressure not exceeding 0.1 kPa at the temperature prescribed in the monograph. high vacuum 高度真空 If other conditions are prescribed, the procedure to be used is described in full in the individual monograph. Appendix III E. Paper Chromatography ■ 色析法示意图： 圆形滤纸 纸层析 展开 Paper partition chromatogra