演示稿(碱性正交图).pptVIP

Electrochemical Behavior of Metal Bipolar Plate Used to DMAFC Yang Chun (Hubei University) Contents Three-Electrode Cell Parameter Background Parameters Setting The Taguchi method Introduction Advantage of The Taguchi method 1、Reducing the variation in a process 2、Produce high quality product at low cost to the manufacturer 3、How different parameters affect the mean and variance of a process 4、Performance characteristic defines how well the process is functioning orthogonal Experimental Design The collection of the necessary data determine factors most affect product quality with a minimum amount of experimentation, thus saving time and resources. The Taguchi method is best used when there is an inter- mediate number of variables (3 to 50), few interactions between variables, and when only a few variables contribute significantly. Method Design of Experiments Orthogonal Experimental Design Linear Sweep Voltammetry (LSV) Experiments 1-3 (LSV) Experiments 4-6 (LSV) Experiments 7-9 (LSV) Parallel Plot (LSV) Amperometric I-t Curve Experiments 1-3 (I-t curve) Experiments 4-6 (I-t curve) Experiments 7-9 (I-t curve) Parallel Plot (I-t curve) Conclusion Plan 1、Evaluation the corrosion resistance performance and service life of SS316L in acid environment 2、Simulated solution of 70℃ 0.5M H2SO4+5ppm –F 3、The open circuit potential - time curves, the potentio- dynamic curves, the chronoamperometry curves were tested in acid environment Three-Electrode Cell 1 Orthogonal Experimental Design 2 Data Testing and Analyses 3 Conclusion and Plan 4 saturated calomel electrode Platinum electrode SS316 working electrode Pt，Hg，Hg2Cl2(s) | Cl-(c) E Θ = 0.2415 V Electrochemical Workstation（CHI600B）