强磁场下烧结MnZn铁氧体-中国有色金属学报.PDF

第 18 卷第 3 期 中国有色金属学报 2008 年 3 月 Vol.18 No.3 The Chinese Journal of Nonferrous Metals Mar. 2008 文章编号：1004-0609(2008)03-0483-06 强磁场下烧结MnZn 铁氧体 傅小明，钟云波，任忠鸣，王 江，邓 康 (上海大学 上海市现代冶金与材料制备重点实验室，上海 200072) 摘 要：将 Fe O 、MnO 和 ZnO 粉末按摩尔比为 52.8׃24.2׃23.0 混合后压制成 30 mm×5 mm×5 mm 的长方条，然 2 3 后在无磁场和 8 T 强磁场下进行烧结，对两种情况下烧结的 MnZn 铁氧体进行 XRD 、SEM 和 VSM 等检测。结果 表明：与无磁场下烧结的 MnZn 铁氧体相比，8 T 强磁场下烧结的 MnZn 铁氧体的(511) 晶面沿平行于磁场方向发 生明显取向，微观形貌也显示明显的取向织构，且致密化程度提高；其磁性能也明显提高，特别是其相对磁导率 提高约 130%；对于强磁场下烧结的 MnZn 铁氧体，平行磁场方向上的饱和磁化强度较垂直磁场方向上的饱和磁 化强度提高 7.56%，而剩余磁化强度降低48.19% 。 关键词：MnZn 铁氧体；强磁场；烧结；取向 中图分类号：O 511.1 文献标识码：A Sintering of MnZn ferrite in high static magnetic field FU Xiao-ming, ZHONG Yun-bo, REN Zhong-ming, WANG Jiang, DENG Kang (Shanghai Key Laboratory of Modern Metallurgy and Material Processing, Shanghai University, Shanghai 200072, China) Abstract: The mixtures of Fe O , MnO and ZnO were sintered without or with 8 T static magnetic field, respectively. 2 3 The sintered MnZn ferrite (MZF) samples in these two cases were characterized by XRD, SEM, VSM and etc. The results show that compared with MZF sintered without magnetic field, (511) plane of MZF sintered in 8 T static magnetic field is strongly oriented along the magnetic field direction. The oriented crystal texture appears in the sample sintered in 8 T static magnetic field, whose density is enhanced remarkably. The magnetic properties are increased. Especially, its relative magnetic permeability along the magnetic field direction is evalua