定性定量分析PVC 材料及其制品的方法（Qualitative and quantitative analysis of PVC material and its products）.docVIP

定性定量分析PVC 材料及其制品的方法（Qualitative and quantitative analysis of PVC material and its products） Infrared quantitative, the key problem is the instrument! With ordinary infrared spectrum, do transmission, the quantity is not sure But the online infrared spectrometer, based on the principle of attenuated total reflection, is quantifiable Now all have formal apparatus come out, mettler sells, other manufacturer also have, oneself on the net check Of course, using a normal spectrograph for full reflection is also inaccurate The infrared can carry out quantitative analysis, and some standard samples are required to compile the macros. The composition analysis in the plastic is often used to qualitatively and quantitatively. After scanning the sample spectrogram, Running macros can get the content of various components. In addition, the infrared quantification is not a very accurate result. If your request is not very good, you can consider it The application of infrared spectroscopy in the quantitative analysis of polyethylene plastics is applied to li jianjun Qualitative and quantitative analysis of PVC material and its products The method of quantitative analysis of PVC material and its products by using infrared spectroscopy and thermogravimetric analysis is introduced in detail. In this paper, the preliminary determination of ir spectra was performed by using pyrolysis method, and the infrared spectrum analysis was verified by dissolution method. PVC material thermal decomposition process more complex, not directly from the testing results of thermogravimetric (TG curve), various components in reading, the test results must be calculated by linear regression equation the content of PVC, PVC content within 35% ~ 80% has good linear relationship (R = 0.9983). Compared with traditional methods of separation and analysis, this method has the advantages of convenience, rapid and accurate analysis. Keywords: infrared spectrum, thermogravimetric analysis, polyvinyl chloride, qu