微波法制备LiFePO4及其电化学性能的研究.pdf

22 5 V ol. 22, N o. 5 2010 5 Chem ica l R esearch and Applica tion M ay, 2010 : 2010 L iFePO 4 1 2 2 3 1* 林 琳 , 马先果 , 郭 勇 , 王 强 , 肖 丹 ( 1, 610065; 2, 610064; 3, 617000 : L iF ePO , X ( XRD ( SEM 4 , , 5% , 01C , 126mA h / g, 50 , 10% , : ; ; ; : O646 : A E lectroch em ical perform ance of L iFePO4 syn thesized by m icrowave processing m ethod 1 2 2 3 1* L in L in , M a X ianguo , Guo Y ong , W ang Q iang , X iao Dan ( 1Co llege of Chem ical Eng inee ring, S ichuan U niversity, Chengdu 610065; 2College o f Chem istry, S ichuan U niversity, Chengdu 610064; 3P anhua Sc ience and T echno logy Co, L td, P anzh ihua 6 17000 A b stract: L iF ePO4 cathode m a terials w ere synthes ized by m icrow ave processing w ith a dom estic m icrow ave ovenT he m ater ia lsw ere character ized by pow e r Xray diffraction and scanning e lectron m icroscopyThe e lectrochem ica l perform ance o f sam ples a t constant m icrow av e pow er w as studied by constant current charged ischarg e expermi entR esu lt ind ica te: the L iF ePO4 / C com po site w ith 5% cabon exh ibited a higher revers ible specific capac ity of 126mA g / g at 01C and show s very stable cycling behav ior K