宝枫叶总黄酮的提取研究.pdfVIP

第25 卷第1 期 食 品 与生 物 技 术学 报 Vol. 25 No . 1 2006 年 1 月 Journal of Food Science and Biotechnology Jan. 2006 : 2006) 元宝枫叶总黄酮的提取研究 * 李云志, 曾凡骏 , 李 帆 ( 四川大学食品学院, 四川成都610065) : 用乙醇作为溶剂, 采用常规浸提法及超 辅助法对元宝枫叶总黄酮的提取进行了对比研 究通过单因素及正交试验结果得到浸提法的优化条件为: 溶剂为体积分数50% 的乙醇溶液, 料 液比1 g 25 mL, 提取时间1. 5 , 浸提温度70 按照此条件提取两次, 第一次提取率94. 16% , 第二次 1. 36%; 超 辅助法的优化条件为: 溶剂为体积分数50% 的乙醇溶液, 料液比1 g 15 mL, 提取时间0. 5 , 浸提温度60 按照此条件提取两次, 第一次提取率为96. 29%, 第二次提取率 为3. 11%. : 元宝枫叶; 总黄酮; 提取; 超声波 : Q 949. 755. 3 : A The Extraction of Flavonoids From the Leaves of A cer tr uncat um Bung e * LI Yunz i, ZENG Fanjun , LI Fan ( Sc ool of Food Science and Engineering, Sic uan Universit y, C engdu 610065, C ina) Abstract:T w o met ods w ere applied to extract flavonoids from t e leaves of Acer truncatum Bunge, t e et anol extraction met ods w it and w it out ltrasonic w ave. T e results of t e ort ogonal experiment s ow ed t e optimum condition of et anol extraction w it out ultrasonic w ave is as follow s: soaking t e raw material w it et anol( 50%, v/ v)w ater solution ( 1 g 25 mL) for 1. 5 at 70 . Under t e same condition, t e raw material w as extracted tw ice. T e extraction rate w as 94. 16% in t e first time, and 1. 36% in t e second time. T e optimum condition of et anol extraction w it ultrasonic w ave w as to soak t e raw material w it et anol ( 50%, v/ v) w ater solution ( 1 g 15 mL) for 0. 5 at 60 . Under t e same condition, t e raw material w as also extracted tw i