固相萃取-高效液相色谱-串联质谱法测定畜禽粪便中的残留抗生素.pdfVIP

第 l0期 王 丽，等：固相萃取高效液相色谱一串联质谱法测定畜禽粪便中的残留抗生素 ·1011· SM2were0．25—7．18，0．15—3．16and0．04~g／kg，respectively．TherecoveriesofTCs，QUs and SM2in pigmanureand chicken dungwere40％ 一124％ atthespikedlevelsfrom 0．1to l0 g／g(RSDsrangedrfom3．0％ to9．5％，n=6)．Themethodwassuccessfullyappliedtodeter— m inetheantibioticsin pigmanure and chicken dungsamples．Themethod hashigh accuracy andsensitivityforthedeterminationofTCs，QUsandSM2inpigmanureandchickendung． Keywords：solidphaseextraction (SPE)；highperformanceliquidchromatography-tandem massspectrometry (HPLC—M