硫酸盐侵蚀混凝土内部硫酸根离子浓度测试方法.pdfVIP

2008年 6月 港 工 技 术 Jun．2008 第 3期 总第 181期 Port Engineering Technology Tota1 181 NO．3 硫酸盐侵蚀混凝土内部 硫酸根离子浓度测试方法 赵顺波 ，陈记豪 ，高润东 ，李庆斌 (1．华北水利水电学院土木与交通学院，河南 郑州 450011； 2．清华大学水科学与工程国家重点实验室，北京 100084) 摘要：在总结现有测试方法的基础上，经过实测验证，提出遭受硫酸盐侵蚀后混凝土由表及里分层硫酸根浓度的一套测 试方法。该方法通过钻取芯样、分层切片并研磨成粉末，精确称量粉末制成试样，然后用改进的硫酸钡重量法测定各试 样中硫酸根离子含量，从而测得混凝土受硫酸盐侵蚀后由表及里的硫酸根离子浓度分布情况和腐蚀深度，为研究硫酸盐 侵蚀混凝土机理研究提供 了测试方法。 关键词：混凝土；硫酸盐侵蚀；硫酸根离子含量；试样制备；改进的硫酸钡重量法 中图分类号：TQ111．14；TU502．5 文献标志码：A 文章编号：1004—9592(2008)03—0031—03 Measurement of Sulfate—ion Content in Concrete Attacked by Sodium Sulfate Zhao Shunbo ，Chen Jihao ，Gao Rundong ，Li Qingbin (1．School of Civil Engineering and Communication，North China University of Water Conservancy and Electric Power，Zhengzhou Henan 45001 1，China；2．State Key Laboratory of Hydroscience and Engineering，Tsinghua University，BeUing 100084，China) Abstract：Based on the current test methods and successfully practice，a set of methods are proposed for measuring the sulfate content in concrete layers from surface to inside attacked by sodium sulfate solu— tion．The main processes include that of drilling the core sample from the specimen，cutting the core sam— pie into slices，pulverizing the slices into powder layer by layer，accurately weighting the powder samples and determining the sulfate—·ion concentrations of every layer samples by the improved barium sulfate gravi-· metric method．Finally，the erosion depth and the distribution of sulfate—ion content in concrete from sur— face tO inside can be known．It provides a test method tO study the mechanism of concrete attacked by sodium sulfate． Key words：concrete；sodium sulfate corrosion；content of sulfate—ion；made of sampl