姜黄挥发油化学成分的分析（Analysis of chemical constituents in essential oil of Curcuma longa）.docVIP

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姜黄挥发油化学成分的分析（Analysis of chemical constituents in essential oil of Curcuma longa）.doc

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姜黄挥发油化学成分的分析（Analysis of chemical constituents in essential oil of Curcuma longa） Analysis of chemical constituents of volatile oil from Curcuma Update: 2009-07-29 Click: Hou Wei Han Suli Wang Hongmei 1 Curcuma longa L. turmeric is the perennial herbaceous, Zingiberaceae turmeric or turmeric rhizome, located in Chinas southern Fujian, Guangdong, Guangxi, Yunnan, Sichuan, Hubei, Shaanxi, Jiangxi, Taiwan and other places. Can be cultivated or wild in plain, mountain grass or bushes. The root of plants (turmeric) also for medicinal. Jiang Huang has choleretic, analgesic and sterilization efficacy. The main active ingredients of volatile oil, glucose, fructose, starch, fatty oil, oxalate etc.. In order to study the composition of volatile oil of Curcuma longa, the root parts of the extraction of volatile oil were determined and analyzed by GC-MS, 51 compounds identified from. 1 materials and sample preparation Jiang Huang bought in Tianjin Chinese medicine store (made in Sichuan), to the skin with wrinkles, and cylindrical section of yellow brown, solid quality is preferred. The plant Curcuma rhizome dry slice, crushed into coarse powder (over 2 sieve) 20 g, the volatile oil extracted from yellow brown volatile oil 2. The root of volatile oil yield is 0.876%. 2 instruments and experimental conditions 2.1 gas chromatographic conditions: GC: SHIMADZU GC-7 gas chromatograph. Using OV-17 capillary column 25 mm * 0.25 mm (UK); sample size: 1 L; carrier gas: N2 (99.99%) (the domestic); pre column pressure: 78.45 kPa, split ratio: 40: 1; inlet temperature: 250 C; temperature programmed conditions: (50 C 8 min), 2 degrees (min), 230 C (16 min). 2.2 MS conditions: British: VG, ZAB-HS, GC-MS-DS mass spectrometry; EI source; ionization chamber temperature: 200 c; ionization voltage: 70 eV; accelerating voltage: 6 kV; resolution: 1000; scanning range: 30 ~ 500 amu; carrier gas: He (99.999%) (Japan); scanning speed 1 s/dec. DS: temperament Spectrum Computer spectrometer (the compute