基于芳基炔醛共轭延伸的1,8-萘酰亚胺的高选择性比色和荧光.PDFVIP

Electronic Supplementary Material (ESI) for Supporting Information for 基于芳基炔醛共轭延伸的1，8-萘酰亚胺的高选择性比色 和荧光氰离子探针 赵飞飞，伍宏伟，刘传祥，毛海舫 （上海应用技术大学化学与环境工程学院，上海201418 ） A selective colorimetric and fluorescent diphenylacetylene-based naphthalimide for sensing of cyanide Feifei Zhao, Hongwei Wu, Chuanxiang Liu* and Haifang Mao* School of Chemical and Environmental Engineering, Shanghai Institute of Technology, Shanghai 20 1418, China * Corresponding authors e-mail: cxliu@sit.edu.cn; mhf@sit.edu.cn 1 13 1. H, C NMR and HRMS-ESI spectrum of the compound 2 (Fig.S1-S3)S3 1 13 2. H, C NMR，HRMS-ESI and IR spectrum of the compound 4 (Fig.S4-S7)S4 3. Fluorescence spectral of chemosensor 4 in CH CN upon the titration with CN (Fig.S8- 3 S9) ……………………………………………………………………………….……….………..S6 - 4.HPLC analysis of chemosensor 4 upon the titration with CN (Fig.S10)………..…S7 - 5. HRMS-ESI spectrum of chemosensor 4 upon the titration with CN (Fig.S11)S9 Experimental sections Unless otherwise noted, solvents and reagents were analytical grade and used without further