毒死蜱在茶叶上的残留消解动态与使用安全性 - 食品安全质量检测学报.pdf

8 4 Vol. 8 No. 4 2017 4 Journal of Food Safety and Quality Apr. , 2017 * 刘腾飞, 董明辉 , 杨代凤, 顾俊荣, 范 君, 孙灵湘 (, 215155) 摘 要: 目的 方法 , 45% 1%, , 结果 0.005~2.0 mg/L , , 0.9990; 0.010.2 1 mg/kg , 81.7%~110.7%, RSD 10%, 0.003 mg/kg0.01 mg/kg540~1080 g/hm2 , , , , , 3.78 d~4.16 d, 21 d, 0.1 mg/kg结论 , (MRL), 45%, 2 1080 g/hm , 1 , 21 d, , 关键词: ; ; ; Residual degradation dynamics and safety of chlorpyrifos used in tea * LIU Teng-Fei, DONG Ming-Hui , YANG Dai-Feng, GU Jun-Rong, FAN Jun, SUN Ling-Xiang (Jiangsu Taihu Area Institute of Agricultural Sciences, Suzhou 215155, China) ABSTRACT: Objective To evaluate the safety of chlorpyrifos sprayed on tea plantation. Methods Residual dynamics of 45% chlorpyrifos EC in tea was studied by using the methods of laboratory test and field trial. Samples were extracted ultrasonically with 1% acetic acid-acetonitrile solution, purified by dispersive solid phase extraction