物相鉴定（Phase identification）.docVIP

物相鉴定（Phase identification） The most fundamental application of X-ray diffraction is the identification of phases. Other applications can only be done after phase identification has been completed. So what is the phase identification? First of all, X ray diffraction method can only prove the existence of a phase, but can not prove the absence of a phase. This is because the X ray diffraction intensity is a statistical result of the sample surface information. When the content of a phase is lower than a lower limit (about 1%-10%, different phase), the XRD method can not test the existence of a phase. So if you want to ask, my sample contains 0.3% of Zr, why can you see it in OM, TEM or SEM, and why cant XRD do it? This question shows that you dont know XRD yet. Secondly, it is not with JADE that it is possible to analyze what is. JADE is a PDF card retrieval program that retrieves basically qualified object cards from the PDF card library by given conditions. But these cards may not be in your sample at all, because some items do not have the corresponding PDF cards. At this time, JADE can do nothing about it. At this point, you can retrieve the cards closest to the actual structure of the object. Third, any search program needs a certain search condition, and JADE is no exception. The diffraction pattern of the sample is itself the most basic retrieval condition, but it is not enough to have the spectrum. The more the known condition, the more accurate the retrieval result is. Heres the search condition, the most used is the element. JADE has three choices. Being, not existing, may exist. People using JADE must really understand how these three situations are used. In the forums, some people give only a map of the data in the help post, hoping that they can help analyze the exact results. To tell you the truth, people are not gods, and you cant tell the fate without telling them any conditions. As a result, spectrum analysis without adding any known conditions often