任慧2012 高温合金中镍含量测定冒高氯酸烟分解有机物的方法研究.pdf

TH83 1 2 Ren Hui ,Zhu Yanrong ,RenYi (1AVIC Beijing Institute of Aeronautical Materials/AVIC Testing Innovation Copperation, Beijing 100095; 2Tianshui Aircraft Industrial Corporation of AVIC, Tianshui 741025) Abstract The determination of Ni in superalloys generally uses the dimethylglyoxime—EDTA volumetric method ( GB and HB).The smoke of perchloric acid to decompose organic substance was described very simply in this method. The detailed operation steps for the smoke of perchloric acid decomposing organic matter, notes and how to test the perchloric acid and so on were not described in detail. The key step on the determination of Ni in superalloy was investigated,it was the smoke of perchloric acid to decompose organic substance.Through survey and analysis, it tested on the soak time about orgainc substance,the volume of perchloric acid,the addtion way and the smoking level. At last it indicated the accurate conclusions and attetions. Key words Superalloy; Nickel; Perchloric acid ρ ρ ρρ ρ