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铌酸钠粉体的水热合成及表征 hydrothermal synthesis of sodium niobate powders
第 期 电 子 元 件 与 材 料
11 Vol.25 No.11
年 月 ELECTRONIC COMPONENTS MATERIALS
2006 11 Nov. 2006
研究与试制研究与试制
研究与试制研究与试制
R D
铌酸钠粉体的水热合成及表征
苗鸿雁 王世平 谈国强
摘要:NaOH Nb O KOH NaNbO
2 5 3
XRD r Na Nb SEM NaNbO3
r Na Nb 4 1 200 NaNbO3
37 nm
关键词:
中图分类号: TB383 O782+ .1 文献标识码:A 文章编号:1001-2028 2006 11-0060-02
Hydrothermal Synthesis of Sodium Niobate Powders
MIAO Hong-yan, WANG Shi-ping, TAN Guo-qiang
(School of Materials Science Engineering, Shanxi University of Science and Technology, Xianyang 712081, China)
Abstract: NaNbO3 microcrystals which are high crystallinity and perfect fine-grains were prepared by hydrothermal method
using Nb O , NaOH as raw materials and KOH as mineralizer. By means of XRD, it was analysed that the factors of Na/Nb and
2 5
the reaction temperature and the reaction time effected on the crystal structure and grain size. And by means of SEM, the
morphology of the prepared NaNbO were studied. The results show that orthorhombic NaNbO microcrystals are synthesized
3 3
when the mole ratio of Na/Nb is 4 1 and the reaction temperature is 200 , at the same time the average grain size is 37 nm.
Key words: inorganic non-metallic materials;sodium niobate; hydrothermal synthesis; orthorhomb
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