精甲醇中水含量的优化控制（Optimal control of water content in refined methanol）.docVIP

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精甲醇中水含量的优化控制（Optimal control of water content in refined methanol）.doc

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精甲醇中水含量的优化控制（Optimal control of water content in refined methanol）

精甲醇中水含量的优化控制（Optimal control of water content in refined methanol） Optimal control of water content in fine methanol Abstract: This paper describes the harm of high water content in methanol product, analyzes the possible causes of the high water content in methanol product and puts forward the solving measures. After verification, the effect is good. Keywords: methanol distillation water content measure I. Introduction Yankuang Cathay Chemical Co. Ltd. is established in 2003 approved high-tech coal chemical enterprises, has a new type of opposedmulti coal water slurry gasification technology and gas power generation two national 863 project. The synthesis of acetic acid by methanol carbonylation with independent intellectual property rights, with the high concentration of carbon monoxide and methanol as raw materials, rhodium iodide as catalyst in the synthesis of acetic acid and heating under pressure. The use of methanol acetic acid methanol synthesis technology developed by Southwest Chemical Industry Research Institute, C307 type low pressure synthesis catalyst. Two, the methanol distillation process The 1. part predistillation tower The expansion tank of crude methanol or methanol synthesis from crude methanol tank to the pre column feed pump pressure after entering the crude methanol steam condensate preheater, by heating to 65 DEG C is transferred into a distillation column. At the top of the methanol steam pre tower condenser after pre column to reflux groove, by pre column reflux pump reflux. The pre part of low boiling point tower condenser group is not condensed and non condensable gas into the non condensable gas condenser cooling to 40 DEG C, the most of the non condensable gas by methanol recovery, pre column pressure regulating valve of sulfur recovery. Pre tower bottom by 0.4MPa steam through the thermosyphon reboiler heat supply. The 2. part pressurized distillation tower Predistillation tower bottom to the pre after methanol by pressurized column